Information card for entry 4075663

Structure parameters

• Formula: C37 H39 Br Cl N O2 P2 Pd
• Calculated formula: C37 H39 Br Cl N O2 P2 Pd
• Title of publication: Synthesis of New Mixed Phosphineσim Iminophosphorane Bidentate Ligands and Their Coordination to Group 10 Metal Centers
• Authors of publication: Boubekeur, Leïla; Ricard, Louis; Mézailles, Nicolas; Le Floch, Pascal
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 6
• Pages of publication: 1065
• a: 9.545 ± 0.001 Å
• b: 10.556 ± 0.001 Å
• c: 18.181 ± 0.001 Å
• α: 93.142 ± 0.001°
• β: 102.686 ± 0.001°
• γ: 106.809 ± 0.001°
• Cell volume: 1697 ± 0.3 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0834
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No