Information card for entry 4075679

Structure parameters

• Formula: C94 H126 O2 P4 Pt2
• Calculated formula: C94 H126 O2 P4 Pt2
• Title of publication: Selective Metallacyclization and Crystallographic Characterization of Structurally Related Platina-annulenes
• Authors of publication: Johnson, Charles A.; Haley, Michael M.; Rather, Elisabeth; Han, Fusen; Weakley, Timothy J. R.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 6
• Pages of publication: 1161
• a: 15.1666 ± 0.0005 Å
• b: 10.3529 ± 0.0003 Å
• c: 28.4724 ± 0.0009 Å
• α: 90°
• β: 104.947 ± 0.001°
• γ: 90°
• Cell volume: 4319.4 ± 0.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0656
• Weighted residual factors for all reflections included in the refinement: 0.0715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No