Information card for entry 4075682

Structure parameters

• Common name: (Salme*)3SiPh*1/2p-Xylene
• Chemical name: Tris-(2-oxyacetophenone-N-methyliminato)phenylsilane p-Xylene solvate
• Formula: C37 H40 N3 O3 Si
• Calculated formula: C37 H40 N3 O3 Si
• Title of publication: Equilibrium between Tetra-, Penta-, and Hexacoordinate Imine and Enamine Chelates of Silicon: Crystal Structure and Variable-Temperature NMR
• Authors of publication: Wagler, Jörg; Böhme, Uwe; Brendler, Erica; Roewer, Gerhard
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 6
• Pages of publication: 1348
• a: 11.889 ± 0.002 Å
• b: 21.871 ± 0.004 Å
• c: 12.464 ± 0.003 Å
• α: 90°
• β: 101.94 ± 0.03°
• γ: 90°
• Cell volume: 3170.8 ± 1.2 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1014
• Weighted residual factors for all reflections included in the refinement: 0.111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No