Information card for entry 4075695

Structure parameters

• Formula: C32 H45 Cl2 Ni O0.5 P2
• Calculated formula: C32 H45 Cl2 Ni O0.5 P2
• Title of publication: Nine-Membered Trans Square-Planar Chelates Formed by a bisbi Analogue
• Authors of publication: Eberhard, Michael R.; Heslop, Katie M.; Orpen, A. Guy; Pringle, Paul G.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 3
• Pages of publication: 335
• a: 10.999 ± 0.005 Å
• b: 20.439 ± 0.006 Å
• c: 27.982 ± 0.008 Å
• α: 88.06 ± 0.03°
• β: 80.25 ± 0.03°
• γ: 74.94 ± 0.03°
• Cell volume: 5986 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1501
• Residual factor for significantly intense reflections: 0.0683
• Weighted residual factors for significantly intense reflections: 0.1264
• Weighted residual factors for all reflections included in the refinement: 0.1542
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No