Information card for entry 4075730

Structure parameters

• Formula: C50 H68 Cl N O P2 Pd
• Calculated formula: C50 H68 Cl N O P2 Pd
• Title of publication: Catalytic Suzuki Coupling Reactions by Amido Phosphine Complexes of Palladium
• Authors of publication: Liang, Lan-Chang; Chien, Pin-Shu; Huang, Mei-Hui
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 3
• Pages of publication: 353
• a: 10.26 ± 0.0002 Å
• b: 12.804 ± 0.0002 Å
• c: 19.634 ± 0.0003 Å
• α: 71.302 ± 0.001°
• β: 87.086 ± 0.001°
• γ: 70.073 ± 0.001°
• Cell volume: 2291.94 ± 0.07 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0506
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1267
• Goodness-of-fit parameter for all reflections included in the refinement: 1.259
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No