Information card for entry 4075861

Structure parameters

• Formula: C38 H34 Cl2 Ge2 N4 O4 W
• Calculated formula: C38 H34 Cl2 Ge2 N4 O4 W
• SMILES: c1(ccccc1)[N]1=C(C)C=C(N(c2ccccc2)[Ge]1([W](C#[O])(C#[O])(C#[O])(C#[O])[Ge]1([N](c2ccccc2)=C(C)C=C(N1c1ccccc1)C)Cl)Cl)C
• Title of publication: In Search of Cationic Germanium(II)−Transition Metal Complexes L2Ge+W(CO)5and L2Ge+W(CO)4Ge+L2
• Authors of publication: Saur, Isabelle; Garcia Alonso, Sonia; Gornitzka, Heinz; Lemierre, Virginie; Chrostowska, Anna; Barrau, Jacques
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 12
• Pages of publication: 2988
• a: 10.4796 ± 0.0014 Å
• b: 9.5423 ± 0.0012 Å
• c: 19.334 ± 0.003 Å
• α: 90°
• β: 103.309 ± 0.002°
• γ: 90°
• Cell volume: 1881.5 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0432
• Residual factor for significantly intense reflections: 0.0275
• Weighted residual factors for significantly intense reflections: 0.0526
• Weighted residual factors for all reflections included in the refinement: 0.0567
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No