Information card for entry 4075869

Structure parameters

• Formula: C31 H48 U
• Calculated formula: C31 H48 U
• Title of publication: Facile Triphenylborane-Based Syntheses of the Sterically Crowded Tris(pentamethylcyclopentadienyl) Complexes (C5Me5)3UMe and (C5Me5)3UCl
• Authors of publication: Evans, William J.; Kozimor, Stosh A.; Ziller, Joseph W.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 14
• Pages of publication: 3407
• a: 10.0075 ± 0.0012 Å
• b: 10.0075 ± 0.0012 Å
• c: 15.452 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 1340.2 ± 0.4 ų
• Cell temperature: 161 ± 2 K
• Ambient diffraction temperature: 161 ± 2 K
• Number of distinct elements: 3
• Space group number: 176
• Hermann-Mauguin space group symbol: P 63/m
• Hall space group symbol: -P 6c
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0603
• Weighted residual factors for all reflections included in the refinement: 0.0719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.263
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No