Information card for entry 4075887

Structure parameters

• Chemical name: Tetrakis{(1,3-diethyl-4,5-dimethyl)imidazolylyliden}nitridotechnetium(V) dichloride'
• Formula: C36 H64 Cl2 N9 Tc
• Calculated formula: C36 H64 Cl2 N9 Tc
• Title of publication: Nitridotechnetium(V) Complexes with N-Heterocyclic Carbenes and Unexpected (OSiMe2OSiMe2O)2-Coligands
• Authors of publication: Braband, Henrik; Abram, Ulrich
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 14
• Pages of publication: 3362
• a: 11.498 ± 0.002 Å
• b: 28.649 ± 0.005 Å
• c: 14.131 ± 0.002 Å
• α: 90°
• β: 94.87 ± 0.02°
• γ: 90°
• Cell volume: 4638 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1059
• Residual factor for significantly intense reflections: 0.0588
• Weighted residual factors for significantly intense reflections: 0.1611
• Weighted residual factors for all reflections included in the refinement: 0.1984
• Goodness-of-fit parameter for all reflections included in the refinement: 0.933
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No