Information card for entry 4075890

Structure parameters

• Formula: C35.5 H52 Cl Mn2 O11 P3 Sn
• Calculated formula: C35.5 H52 Cl Mn2 O11 P3 Sn
• Title of publication: Phosphonate−Stannylene Coupling in the Reactions of the Anion [Mn2{μ-OP(OEt)2}{μ-P(OEt)2}(CO)6]2-with SnR2Cl2(R = Bu, Ph)
• Authors of publication: Liu, Xiang-Yang; Ruiz, Miguel A.; Lanfranchi, Maurizio; Tiripicchio, Antonio
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 14
• Pages of publication: 3527
• a: 12.367 ± 0.004 Å
• b: 20.625 ± 0.005 Å
• c: 35.067 ± 0.007 Å
• α: 90°
• β: 91.24 ± 0.02°
• γ: 90°
• Cell volume: 8942 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1332
• Residual factor for significantly intense reflections: 0.0669
• Weighted residual factors for significantly intense reflections: 0.181
• Weighted residual factors for all reflections included in the refinement: 0.2217
• Goodness-of-fit parameter for all reflections included in the refinement: 1.153
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No