Crystallography Open Database

Information card for entry 4075939

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Coordinates	4075939.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H53 N Ru3
Calculated formula	C37 H38 N Ru3
Title of publication	Synthesis and Structure of a Triruthenium Complex Containing a Perpendicularly Coordinatedμ3-η2:η2(⊥)-Nitrile Ligand and Its Protonation To Yield a Perpendicularly Coordinated Iminoacyl Ligand
Authors of publication	Takao, Toshiro; Kawashima, Takashi; Matsubara, Kouki; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	14
Pages of publication	3371
a	17.354 ± 0.002 Å
b	18.293 ± 0.003 Å
c	11.311 ± 0.002 Å
α	90°
β	106.663 ± 0.007°
γ	90°
Cell volume	3440 ± 0.9 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0405
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.0992
Weighted residual factors for all reflections included in the refinement	0.1006
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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