Crystallography Open Database

Information card for entry 4075984

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Coordinates	4075984.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 Os Ru
Calculated formula	C24 H30 Os Ru
Title of publication	Heterobimetallic Polyhydride Complex, CpRu(μ-H)4OsCp (Cp* = η5-C5Me5). Synthesis and Reaction with Ethylene
Authors of publication	Shima, Takanori; Suzuki, Hiroharu
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	16
Pages of publication	3939
a	6.8764 ± 0.0006 Å
b	8.6346 ± 0.0006 Å
c	10.6228 ± 0.0015 Å
α	102.12 ± 0.006°
β	104.308 ± 0.005°
γ	108.693 ± 0.003°
Cell volume	549.44 ± 0.1 Å³
Cell temperature	243 ± 2 K
Ambient diffraction temperature	243 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0234
Residual factor for significantly intense reflections	0.0226
Weighted residual factors for significantly intense reflections	0.0548
Weighted residual factors for all reflections included in the refinement	0.0552
Goodness-of-fit parameter for all reflections included in the refinement	1.163
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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