Information card for entry 4076026

Structure parameters

• Formula: C8 H22 F I N2 Pt
• Calculated formula: C8 H22 F I0.886 N2 Pt
• Title of publication: Unexpected Formation of an Organoplatinum(IV) Fluoride Complex in the Reaction of Pt(TMEDA)(CH3)2with Perfluoro-sec-butyl Iodide
• Authors of publication: Hughes, Russell P.; Laritchev, Roman B.; Zakharov, Lev N.; Rheingold, Arnold L.
• Journal of publication: Organometallics
• Year of publication: 2005
• Journal volume: 24
• Journal issue: 20
• Pages of publication: 4845
• a: 12.364 ± 0.002 Å
• b: 13.339 ± 0.002 Å
• c: 7.8955 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1302.2 ± 0.4 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.0688
• Weighted residual factors for all reflections included in the refinement: 0.0699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.173
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No