Crystallography Open Database

Information card for entry 4076177

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Coordinates	4076177.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H84 Lu2 N2 O2
Calculated formula	C58 H82 Lu2 N2 O2
Title of publication	The Elusive (C5Me4H)3Lu: Its Synthesis and LnZ3/K/N2Reactivity
Authors of publication	Evans, William J.; Lee, David S.; Johnston, Matthew A.; Ziller, Joseph W.
Journal of publication	Organometallics
Year of publication	2005
Journal volume	24
Journal issue	26
Pages of publication	6393
a	15.123 ± 0.005 Å
b	13.951 ± 0.005 Å
c	25.662 ± 0.008 Å
α	90°
β	105.263 ± 0.005°
γ	90°
Cell volume	5223 ± 3 Å³
Cell temperature	163 ± 2 K
Ambient diffraction temperature	163 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0491
Residual factor for significantly intense reflections	0.0439
Weighted residual factors for significantly intense reflections	0.1326
Weighted residual factors for all reflections included in the refinement	0.1362
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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