Information card for entry 4076490

Structure parameters

• Common name: LH.AlCl3
• Formula: C54 H80 Al2 Cl6 N4 O3
• Calculated formula: C54 H80 Al2 Cl6 N4 O3
• Title of publication: Syntheses and Reactions of Derivatives of (Pyrrolylaldiminato)germanium(II) and -Aluminum(III)
• Authors of publication: Yang, Ying; Zhao, Na; Zhu, Hongping; Roesky, Herbert W.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 1958
• a: 9.7417 ± 0.0002 Å
• b: 18.6543 ± 0.0005 Å
• c: 17.6245 ± 0.0005 Å
• α: 90°
• β: 102.034 ± 0.003°
• γ: 90°
• Cell volume: 3132.42 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0723
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.1232
• Weighted residual factors for all reflections included in the refinement: 0.1317
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No