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Information card for entry 4076507
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Coordinates | 4076507.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H53 B2 F4 N6 O2 Os P |
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Calculated formula | C33 H53 B2 F4 N6 O2 Os P |
Title of publication | Anti-Markovnikov 1,3-CH Addition of Allenes to Allenes: A Straightforward Method To Prepare Osmium‒Dienylcarbene Complexes |
Authors of publication | Castro-Rodrigo, Ruth; Esteruelas, Miguel A.; López, Ana M.; Oñate, Enrique |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 5 |
Pages of publication | 1991 |
a | 12.2995 ± 0.0016 Å |
b | 16.471 ± 0.002 Å |
c | 18.697 ± 0.002 Å |
α | 90° |
β | 99.903 ± 0.002° |
γ | 90° |
Cell volume | 3731.3 ± 0.8 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.099 |
Residual factor for significantly intense reflections | 0.0433 |
Weighted residual factors for significantly intense reflections | 0.0872 |
Weighted residual factors for all reflections included in the refinement | 0.1063 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.019 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4076507.html
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structural data.