Information card for entry 4076537

Structure parameters

• Formula: C36 H82 Cl2 N4 P2 Si8 Sn2
• Calculated formula: C36 H82 Cl2 N4 P2 Si8 Sn2
• SMILES: C[Si](C)(C)N([Si](C)(C)C)[Sn](P(P(c1ccccc1)[Sn](N([Si](C)(C)C)[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)Cl)c1ccccc1)(N([Si](C)(C)C)[Si](C)(C)C)Cl
• Title of publication: Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
• Authors of publication: West, Joseph K.; Stahl, Lothar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2042
• a: 9.5087 ± 0.001 Å
• b: 10.5988 ± 0.0011 Å
• c: 15.3895 ± 0.0015 Å
• α: 75.362 ± 0.002°
• β: 78.652 ± 0.002°
• γ: 70.747 ± 0.001°
• Cell volume: 1405.7 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0267
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0669
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No