Information card for entry 4076539

Structure parameters

• Formula: C24 H46 Cl Ge N2 P Si4
• Calculated formula: C24 H46 Cl Ge N2 P Si4
• SMILES: [Ge](Cl)(P(c1ccccc1)c1ccccc1)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
• Authors of publication: West, Joseph K.; Stahl, Lothar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2042
• a: 9.01 ± 0.001 Å
• b: 11.5526 ± 0.0013 Å
• c: 17.337 ± 0.002 Å
• α: 89.039 ± 0.002°
• β: 78.051 ± 0.002°
• γ: 67.828 ± 0.002°
• Cell volume: 1631.2 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0405
• Residual factor for significantly intense reflections: 0.0342
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0922
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No