Information card for entry 4076542

Structure parameters

• Formula: C16 H45 Cl2 Ge N2 P Si4
• Calculated formula: C16 H45 Cl2 Ge N2 P Si4
• SMILES: [Ge](Cl)(P(Cl)C(C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Insertions of Cyclic and Acyclic Germanium and Tin Heterocarbenoids into Phosphorus‒Chlorine Bonds: Syntheses, Structures, and Reactivities
• Authors of publication: West, Joseph K.; Stahl, Lothar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2042
• a: 10.6676 ± 0.0009 Å
• b: 11.8453 ± 0.001 Å
• c: 12.1007 ± 0.0011 Å
• α: 77.3 ± 0.001°
• β: 89.967 ± 0.001°
• γ: 76.158 ± 0.001°
• Cell volume: 1446.1 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0237
• Residual factor for significantly intense reflections: 0.0226
• Weighted residual factors for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections included in the refinement: 0.0655
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No