Information card for entry 4076580

Structure parameters

• Formula: C20 H34 Ge2 N4
• Calculated formula: C20 H34 Ge2 N4
• SMILES: [Ge]1N(c2c(cc3N([Ge]N(c3c2)CC(C)(C)C)CC(C)(C)C)N1CC)CC
• Title of publication: Synthesis and Characterization of Rigid Ditopic N-Heterocyclic Benzobisgermylenes and -stannylenes
• Authors of publication: Krupski, Sergei; Dickschat, Julia V.; Hepp, Alexander; Pape, Tania; Hahn, F. Ekkehardt
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 5
• Pages of publication: 2078
• a: 16.9241 ± 0.0017 Å
• b: 5.9332 ± 0.0006 Å
• c: 22.483 ± 0.002 Å
• α: 90°
• β: 102.826 ± 0.002°
• γ: 90°
• Cell volume: 2201.3 ± 0.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0765
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.077
• Weighted residual factors for all reflections included in the refinement: 0.0894
• Goodness-of-fit parameter for all reflections included in the refinement: 0.98
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No