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Information card for entry 4076594
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Coordinates | 4076594.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | [K(2,2,2-crypt)]{P[C(NHDipp)(NDipp)][C(NHiPr)(NiPr)]}*hex |
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Formula | C56 H100 K N6 O6 P7 |
Calculated formula | C56 H100 K N6 O6 P7 |
Title of publication | Hydrophosphination of Carbodiimides Using Protic Heptaphosphide Cages: A Unique Effect of the Bimodal Activity of Protonated Group 15 Zintl Ions |
Authors of publication | Turbervill, Robert S. P.; Goicoechea, Jose M. |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 6 |
Pages of publication | 2452 |
a | 15.9418 ± 0.0002 Å |
b | 16.7687 ± 0.0002 Å |
c | 26.4606 ± 0.0004 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 7073.53 ± 0.16 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0729 |
Residual factor for significantly intense reflections | 0.0631 |
Weighted residual factors for significantly intense reflections | 0.1699 |
Weighted residual factors for all reflections included in the refinement | 0.1799 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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