Information card for entry 4076645

Structure parameters

• Formula: C47 H58 N3 Yb
• Calculated formula: C47 H58 N3 Yb
• Title of publication: Synthesis, Reactivity, and Structure of Mixed-Ligand Ytterbium Complexes Supported by β-Diketiminate
• Authors of publication: Yao, Yingming; Zhang, Yong; Shen, Qi; Yu, Kaibei
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 5
• Pages of publication: 819
• a: 12.42 ± 0.002 Å
• b: 16.469 ± 0.003 Å
• c: 40.264 ± 0.007 Å
• α: 90°
• β: 93.53 ± 0.01°
• γ: 90°
• Cell volume: 8220 ± 2 ų
• Cell temperature: 290 ± 2 K
• Ambient diffraction temperature: 290 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1147
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0815
• Goodness-of-fit parameter for all reflections included in the refinement: 0.816
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No