Crystallography Open Database

Information card for entry 4076655

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Coordinates	4076655.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C164 H146 Cl4 O11 P4 Pd2
Calculated formula	C160 Cl4 O8 P4 Pd2
Title of publication	Platinum(II) and Palladium(II) Complexes of Bis(diphenylphosphino)calix[4]arene Tetrabenzyl Ether: Fluxional Behavior Caused by Two Motions
Authors of publication	Takenaka, Kazuhiro; Obora, Yasushi; Jiang, Li Hong; Tsuji, Yasushi
Journal of publication	Organometallics
Year of publication	2002
Journal volume	21
Journal issue	6
Pages of publication	1158
a	17.687 ± 0.0001 Å
b	17.9715 ± 0.0003 Å
c	13.0832 ± 0.0003 Å
α	96.711 ± 0.001°
β	106.965 ± 0.001°
γ	114.131 ± 0.002°
Cell volume	3494.72 ± 0.13 Å³
Cell temperature	96.1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.097
Weighted residual factors for all reflections included in the refinement	0.133
Goodness-of-fit parameter for all reflections included in the refinement	1.759
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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