Crystallography Open Database

Information card for entry 4076670

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Coordinates	4076670.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41.5 H28 Cl O7 Os3 Sb
Calculated formula	C41.5 H28 Cl O7 Os3 Sb
Title of publication	Reactions of the Triosmium−Antimony Cluster Os3(μ-SbPh2)(μ-H)(μ3,η2-C6H4)(CO)9with Alkynes: C−C Bond Coupling to a Cluster-Bound Phenylene and Catalytic Alkyne Cyclotrimerization
Authors of publication	Deng, Mingli; Leong, Weng Kee
Journal of publication	Organometallics
Year of publication	2002
Journal volume	21
Journal issue	6
Pages of publication	1221
a	9.2354 ± 0.0001 Å
b	10.0936 ± 0.0002 Å
c	22.8557 ± 0.0004 Å
α	101.084 ± 0.001°
β	97.728 ± 0.001°
γ	97.503 ± 0.001°
Cell volume	2044.86 ± 0.06 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0556
Residual factor for significantly intense reflections	0.0369
Weighted residual factors for significantly intense reflections	0.0735
Weighted residual factors for all reflections included in the refinement	0.0808
Goodness-of-fit parameter for all reflections included in the refinement	1.056
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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