Information card for entry 4076673

Structure parameters

• Formula: C40.5 H28.5 O7 Os3 Sb
• Calculated formula: C40.5 H28.5 O7 Os3 Sb
• Title of publication: Reactions of the Triosmium−Antimony Cluster Os3(μ-SbPh2)(μ-H)(μ3,η2-C6H4)(CO)9with Alkynes: C−C Bond Coupling to a Cluster-Bound Phenylene and Catalytic Alkyne Cyclotrimerization
• Authors of publication: Deng, Mingli; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 6
• Pages of publication: 1221
• a: 9.3913 ± 0.0001 Å
• b: 13.521 ± 0.0001 Å
• c: 16.7683 ± 0.0002 Å
• α: 82.149 ± 0.001°
• β: 85.3°
• γ: 72.68°
• Cell volume: 2011.72 ± 0.04 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0893
• Weighted residual factors for all reflections included in the refinement: 0.0967
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No