Information card for entry 4076758

Structure parameters

• Common name: [SnF(CH2C6H5){(C(SiMe3)2SiMe2CH2CH2SiMe2C(SiMe3)2}]
• Formula: C27 H59 F4 Si6 Sn
• Calculated formula: C27 H57.284 F Si6 Sn
• Title of publication: Reactions of a Highly Crowded Triorganotin Iodide with Silver Salts. Migration of a Methyl Group from Silicon to Tin within a Cation
• Authors of publication: Asadi, Ashrafolmolouk; Avent, Anthony G.; Eaborn, Colin; Hill, Michael S.; Hitchcock, Peter B.; Meehan, Margaret M.; Smith, J. David
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 11
• Pages of publication: 2183
• a: 9.3336 ± 0.0003 Å
• b: 19.3177 ± 0.0009 Å
• c: 20.2094 ± 0.0009 Å
• α: 91.816 ± 0.002°
• β: 94.81 ± 0.003°
• γ: 94.102 ± 0.002°
• Cell volume: 3619.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No