Information card for entry 4076819

Structure parameters

• Formula: C76.78 H77.56 B22 Br12 Cl5.56 P4 Rh2
• Calculated formula: C76.78 H72 B22 Br12 Cl5.56 P4 Rh2
• Title of publication: Rhodium Phosphines Partnered with the Carborane Monoanions [CB11H6Y6]-(Y = H, Br). Synthesis and Evaluation as Alkene Hydrogenation Catalysts
• Authors of publication: Rifat, Adem; Patmore, Nathan J.; Mahon, Mary F.; Weller, Andrew S.
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 14
• Pages of publication: 2856
• a: 26.957 ± 0.0006 Å
• b: 15.029 ± 0.0004 Å
• c: 27.897 ± 0.0007 Å
• α: 90°
• β: 113.284 ± 0.002°
• γ: 90°
• Cell volume: 10381.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1249
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for significantly intense reflections: 0.1246
• Weighted residual factors for all reflections included in the refinement: 0.1465
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No