Information card for entry 4076947

Structure parameters

• Formula: C24 H39 B2 O7 P
• Calculated formula: C24 H39 B2 O7 P
• Title of publication: Platinum(0)-Catalyzed Diboration of Alkynylboronates and Alkynylphosphonates with Bis(pinacolato)diborane(4): Molecular Structures of [((Me4C2O2)B)(C6H5)CC(P(O)(OC2H5)2)(B(O2C2Me4))] and [((Me4C2O2)B)(C4H9)CC(B(O2C2Me4))2]
• Authors of publication: Ali, Hijazi Abu; El Aziz Al Quntar, Abed; Goldberg, Israel; Srebnik, Morris
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 21
• Pages of publication: 4533
• a: 10.284 ± 0.0002 Å
• b: 11.917 ± 0.0002 Å
• c: 21.77 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2668.01 ± 0.09 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0877
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1407
• Weighted residual factors for all reflections included in the refinement: 0.1599
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No