Crystallography Open Database

Information card for entry 4076954

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Coordinates	4076954.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H37 B Br Cl4 N2 O Os P2
Calculated formula	C43.5 H37 B Br Cl4 N2 O Os P2
Title of publication	Tethered Boryl and Base-Stabilized Borylene Osmium Complexes from the Reaction of Os(BCl2)Cl(CO)(PPh3)2with 2-Aminopyridine
Authors of publication	Rickard, Clifton E. F.; Roper, Warren R.; Williamson, Alex; Wright, L. James
Journal of publication	Organometallics
Year of publication	2002
Journal volume	21
Journal issue	22
Pages of publication	4862
a	26.0038 ± 0.0003 Å
b	19.2065 ± 0.0003 Å
c	17.2856 ± 0.0002 Å
α	90°
β	100.016 ± 0.001°
γ	90°
Cell volume	8501.58 ± 0.19 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	9
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0609
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.1131
Weighted residual factors for all reflections included in the refinement	0.1226
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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