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Information card for entry 4076958
Preview
Coordinates | 4076958.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C43 H38 B Cl N2 O Os P2 |
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Calculated formula | C43 H38 B Cl N2 O Os P2 |
SMILES | [OsH]1([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)([N](=C2N(B1Cl)C=CC=C2)C)C#[O] |
Title of publication | Tethered Boryl and Base-Stabilized Borylene Osmium Complexes from the Reaction of Os(BCl2)Cl(CO)(PPh3)2with 2-Aminopyridine |
Authors of publication | Rickard, Clifton E. F.; Roper, Warren R.; Williamson, Alex; Wright, L. James |
Journal of publication | Organometallics |
Year of publication | 2002 |
Journal volume | 21 |
Journal issue | 22 |
Pages of publication | 4862 |
a | 9.3471 ± 0.0005 Å |
b | 12.4256 ± 0.0006 Å |
c | 16.8918 ± 0.0008 Å |
α | 83.745 ± 0.001° |
β | 85.689 ± 0.001° |
γ | 75.116 ± 0.001° |
Cell volume | 1882.48 ± 0.16 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.034 |
Residual factor for significantly intense reflections | 0.027 |
Weighted residual factors for significantly intense reflections | 0.0567 |
Weighted residual factors for all reflections included in the refinement | 0.0598 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4076958.html
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