Information card for entry 4077029

Structure parameters

• Common name: RuTp(=CCH2C6H9-apic)Cl.O(C2H5)2 = (3c.O(C2H5)2)
• Formula: C27 H38 B Cl N8 O Ru
• Calculated formula: C27 H38 B Cl N8 O Ru
• Title of publication: Ruthenium Trispyrazolylborate Complexes. 18.1Aminocarbene Ruthenium Complexes Derived from Terminal Alkynes and 2-Aminopyridines
• Authors of publication: Rüba, Eva; Hummel, Alexandra; Mereiter, Kurt; Schmid, Roland; Kirchner, Karl
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 23
• Pages of publication: 4955
• a: 11.1834 ± 0.0014 Å
• b: 11.2476 ± 0.0015 Å
• c: 13.0811 ± 0.0017 Å
• α: 112.451 ± 0.002°
• β: 95.864 ± 0.002°
• γ: 101.221 ± 0.002°
• Cell volume: 1463.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0725
• Weighted residual factors for all reflections included in the refinement: 0.0743
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No