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Information card for entry 4077066
Preview
Coordinates | 4077066.cif |
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Original paper (by DOI) | HTML |
Formula | C44.67 H72 O17.33 P5.33 Sn2.67 |
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Calculated formula | C44.6667 H72 O17.3333 P5.33333 Sn2.66667 |
Title of publication | Synthesis of a Tetranuclear Organooxotin Cage by Debenzylation Reactions: X-ray Crystal Structure of [(PhCH2)2Sn2O(O2P(OH)-t-Bu)4]2 |
Authors of publication | Chandrasekhar, Vadapalli; Baskar, Viswanathan; Steiner, Alexander; Zacchini, Stefano |
Journal of publication | Organometallics |
Year of publication | 2002 |
Journal volume | 21 |
Journal issue | 21 |
Pages of publication | 4528 |
a | 21.774 ± 0.004 Å |
b | 24.507 ± 0.005 Å |
c | 16.699 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 8911 ± 3 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 5 |
Space group number | 52 |
Hermann-Mauguin space group symbol | P n n a |
Hall space group symbol | -P 2a 2bc |
Residual factor for all reflections | 0.041 |
Residual factor for significantly intense reflections | 0.0233 |
Weighted residual factors for significantly intense reflections | 0.0649 |
Weighted residual factors for all reflections included in the refinement | 0.072 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.082 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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