Information card for entry 4077329

Structure parameters

• Formula: C66 H57 N2 O5 P4 Ru2
• Calculated formula: C66 H57 N2 O5 P4 Ru2
• Title of publication: Synthesis and Reactivity of a Diruthenium Diazoalkane Complex
• Authors of publication: Gao, Yuan; Jennings, Michael C.; Puddephatt, Richard J.; Jenkins, Hilary A.
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 16
• Pages of publication: 3500
• a: 15.1244 ± 0.0006 Å
• b: 15.1244 ± 0.0006 Å
• c: 28.291 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6471.5 ± 0.5 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 96
• Hermann-Mauguin space group symbol: P 43 21 2
• Hall space group symbol: P 4nw 2abw
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.1495
• Weighted residual factors for all reflections included in the refinement: 0.1602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No