Information card for entry 4077378

Structure parameters

• Formula: C87 H80 B2 Cl4 F40 Ir2 P2 Si2
• Calculated formula: C90.44 H64 B2 Cl2.81 F40 Ir2 P2 Si2
• Title of publication: An Observable Silene/Silylene Rearrangement in a Cationic Iridium Complex
• Authors of publication: Klei, Steven R.; Tilley, T. Don; Bergman, Robert G.
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 15
• Pages of publication: 3220
• a: 13.9503 ± 0.0007 Å
• b: 17.4048 ± 0.0009 Å
• c: 22.577 ± 0.001 Å
• α: 110.337 ± 0.001°
• β: 91.31 ± 0.001°
• γ: 100.383 ± 0.001°
• Cell volume: 5034.1 ± 0.4 ų
• Cell temperature: 171.2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections included in the refinement: 0.0718
• Goodness-of-fit parameter for all reflections included in the refinement: 2.16
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No