Information card for entry 4077409

Structure parameters

• Formula: C14 H29 B N4 Si
• Calculated formula: C14 H29 B N4 Si
• SMILES: [Si](C(=N#N)B1N(C=CN1C(C)(C)C)C(C)(C)C)(C)(C)C
• Title of publication: Synthesis and Structure of Stable α-Boranyldiazomethanes: 1,3-Di-tert-butyl-2,3-dihydro-1H-1,3,2-diazaborolyl- (trimethylsilyl)diazomethane and 1,3-diethyl-2,3-dihydro-1H-1,3,2-benzodiazaborolyl- (trimethylsilyl)diazomethane
• Authors of publication: Weber, Lothar; Wartig, Henning B.; Stammler, Hans-Georg; Neumann, Beate
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 24
• Pages of publication: 5248
• a: 8.973 ± 0.0001 Å
• b: 9.866 ± 0.0001 Å
• c: 11.337 ± 0.0002 Å
• α: 93.553 ± 0.0005°
• β: 90.072 ± 0.0005°
• γ: 115.338 ± 0.0005°
• Cell volume: 904.91 ± 0.02 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.099
• Weighted residual factors for all reflections included in the refinement: 0.1052
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No