Information card for entry 4077411

Structure parameters

• Formula: C36 H52 Ge2
• Calculated formula: C36 H52 Ge2
• SMILES: [Ge]([Ge](C(C)(C)C)(C(C)(C)C)C(C)(C)C)c1c(cccc1c1c(cc(cc1C)C)C)c1c(cc(cc1C)C)C
• Title of publication: Synthesis and Structure of Stable Tri-tert-butylgermyl-Substituted Stannylene and Germylene
• Authors of publication: Setaka, Wataru; Sakamoto, Kenkichi; Kira, Mitsuo; Power, Philip P.
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 22
• Pages of publication: 4460
• a: 10.9715 ± 0.001 Å
• b: 18.445 ± 0.0016 Å
• c: 16.3004 ± 0.0014 Å
• α: 90°
• β: 90.979 ± 0.002°
• γ: 90°
• Cell volume: 3298.2 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.0467
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1249
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No