Information card for entry 4077527

Structure parameters

• Formula: C26 H30 As4 O6 W4
• Calculated formula: C26 H30 As4 O6 W4
• Title of publication: Novel Approach to Intermediates Containing a Tungsten−Arsenic Triple Bond†
• Authors of publication: Johnson, Brian P.; Schiffer, Michael; Scheer, Manfred
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 17
• Pages of publication: 3404
• a: 10.18 ± 0.002 Å
• b: 16.34 ± 0.003 Å
• c: 19.866 ± 0.004 Å
• α: 90°
• β: 97.73 ± 0.03°
• γ: 90°
• Cell volume: 3274.5 ± 1.1 ų
• Cell temperature: 200 ± 1 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.055
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0945
• Weighted residual factors for all reflections included in the refinement: 0.1046
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No