Information card for entry 4077569

Structure parameters

• Formula: C49 H27 B F24 Mn O7 P
• Calculated formula: C49 H27 B F24 Mn O7 P
• Title of publication: Synthesis of and Small Molecule Coordination to Highly Electrophilic Cationic Manganese(I) and Rhenium(I) Carbonyl Complexes with Tied-Back Phosphites
• Authors of publication: Fang, Xinggao; Scott, Brian L.; John, Kevin D.; Kubas, Gregory J.
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 20
• Pages of publication: 4141
• a: 18.1505 ± 0.0009 Å
• b: 14.6079 ± 0.0007 Å
• c: 21.074 ± 0.001 Å
• α: 90°
• β: 101.339 ± 0.001°
• γ: 90°
• Cell volume: 5478.5 ± 0.5 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0826
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.1761
• Weighted residual factors for all reflections included in the refinement: 0.1948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No