Information card for entry 4077664

Structure parameters

• Chemical name: iodo-carbonyl-(eta$6!-p-cymene)-bis-(mu!2$-pyrazolyl-N,N')- rhodium(i)-osmium(ii)
• Formula: C17 H20 I N4 O Os Rh
• Calculated formula: C17 H20 I N4 O Os Rh
• Title of publication: Synthesis, Characterization, and Theoretical Studies on Heterobinuclear (p-cymene)Os(μ-pz)2M (M = Ir, Rh; Hpz = Pyrazole) Complexes
• Authors of publication: Carmona, Daniel; Ferrer, Joaquina; Arilla, José M.; Reyes, Josefa; Lahoz, Fernando J.; Elipe, Sergio; Modrego, F. Javier; Oro, Luis A.
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 5
• Pages of publication: 798
• a: 9.2213 ± 0.0015 Å
• b: 13.577 ± 0.002 Å
• c: 16.009 ± 0.002 Å
• α: 90°
• β: 102.544 ± 0.012°
• γ: 90°
• Cell volume: 1956.4 ± 0.5 ų
• Cell temperature: 200 ± 0.2 K
• Ambient diffraction temperature: 200 ± 0.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0809
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.06
• Weighted residual factors for all reflections included in the refinement: 0.0675
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No