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Information card for entry 4077733
Preview
Coordinates | 4077733.cif |
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Original paper (by DOI) | HTML |
Formula | C12 H21 Cl2 N O3 Ti |
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Calculated formula | C12 H21 Cl2 N O3 Ti |
Title of publication | N-Alkoxy-β-ketoiminate Complexes of Groups 4 and 5: Synthesis and Characterization of the Complexes [(η5-C5H4R)M{CH3C(O)CHC(NCH2CHR‘O)CH3}Cln] (M = Ti,n= 1; M = Nb,n= 2; R = H, Me; R‘ = H, Me), [Ti{CH3C(O)CHC(NCH2CHR‘O)CH3}Cl2(thf)], and [Ti{CH3C(O)CHC(NCH2CHR‘O)CH3}2] |
Authors of publication | Doherty, Simon; Errington, R. John; Housley, Neil; Ridland, John; Clegg, William; Elsegood, Mark R. J. |
Journal of publication | Organometallics |
Year of publication | 1999 |
Journal volume | 18 |
Journal issue | 6 |
Pages of publication | 1018 |
a | 14.4022 ± 0.0009 Å |
b | 14.6208 ± 0.0009 Å |
c | 14.8973 ± 0.0009 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3136.9 ± 0.3 Å3 |
Cell temperature | 160 ± 2 K |
Ambient diffraction temperature | 160 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0641 |
Residual factor for significantly intense reflections | 0.0457 |
Weighted residual factors for significantly intense reflections | 0.0949 |
Weighted residual factors for all reflections included in the refinement | 0.1037 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.07 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4077733.html
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