Information card for entry 4077772

Structure parameters

• Formula: C23.85 H21.57 Cl0.14 N2 O Pd
• Calculated formula: C23.8555 H21.5665 Cl0.1445 N2 O Pd
• Title of publication: Periphery-Palladated Carbosilane Dendrimers: Synthesis and Reactivity of Organopalladium(II) and -(IV) Dendritic Complexes. Crystal Structure of [PdMe(C6H4(OCH2Ph)-4)(bpy)] (bpy = 2,2‘-Bipyridine)
• Authors of publication: Hovestad, Neldes J.; Hoare, Jason L.; Jastrzebski, Johann T. B. H.; Canty, Allan J.; Smeets, Wilberth J. J.; Spek, Anthony L.; van Koten, Gerard
• Journal of publication: Organometallics
• Year of publication: 1999
• Journal volume: 18
• Journal issue: 16
• Pages of publication: 2970
• a: 10.6985 ± 0.0008 Å
• b: 11.8973 ± 0.0008 Å
• c: 17.5225 ± 0.0014 Å
• α: 103.495 ± 0.006°
• β: 92.797 ± 0.006°
• γ: 114.671 ± 0.008°
• Cell volume: 1943.6 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1257
• Residual factor for significantly intense reflections: 0.0592
• Weighted residual factors for all reflections: 0.1356
• Weighted residual factors for significantly intense reflections: 0.1115
• Goodness-of-fit parameter for all reflections: 0.998
• Goodness-of-fit parameter for significantly intense reflections: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No