Information card for entry 4077812

Structure parameters

• Formula: C26 H24 Ge2
• Calculated formula: C26 H24 Ge2
• Title of publication: Homo- and Cross-[2+2]-Cycloaddition of 1,1-Diphenylsilene and 1,1-Diphenylgermene. Absolute Rate Constants for Dimerization and the Molecular Structures and Photochemistry of the Resulting 1,3-Dimetallacyclobutanes
• Authors of publication: Toltl, Nicholas P.; Stradiotto, Mark; Morkin, Tracy L.; Leigh, William J.
• Journal of publication: Organometallics
• Year of publication: 1999
• Journal volume: 18
• Journal issue: 26
• Pages of publication: 5643
• a: 10.2432 ± 0.0002 Å
• b: 10.5455 ± 0.0001 Å
• c: 11.3542 ± 0.0001 Å
• α: 103.452 ± 0.001°
• β: 102.52°
• γ: 93.074 ± 0.001°
• Cell volume: 1157.45 ± 0.03 ų
• Cell temperature: 300 ± 2 K
• Ambient diffraction temperature: 300 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.037
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for all reflections: 0.0737
• Weighted residual factors for significantly intense reflections: 0.0693
• Goodness-of-fit parameter for all reflections: 1.037
• Goodness-of-fit parameter for significantly intense reflections: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No