Information card for entry 4077840

Structure parameters

• Formula: C52 H83 B O4 Os P2
• Calculated formula: C52 H83 B O4 Os P2
• Title of publication: Reactions of Osmium‒Pinacolboryl Complexes: Preparation of the First Vinylideneboronate Esters
• Authors of publication: Esteruelas, Miguel A.; López, Ana M.; Mora, Malka; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 2965
• a: 11.0486 ± 0.0006 Å
• b: 24.2722 ± 0.0014 Å
• c: 18.719 ± 0.0011 Å
• α: 90°
• β: 90.188 ± 0.001°
• γ: 90°
• Cell volume: 5019.9 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0339
• Weighted residual factors for significantly intense reflections: 0.0786
• Weighted residual factors for all reflections included in the refinement: 0.0823
• Goodness-of-fit parameter for all reflections included in the refinement: 0.96
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No