Crystallography Open Database

Information card for entry 4077902

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Coordinates	4077902.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83 H65 B F24 O P3 Rh
Calculated formula	C83 H65 B F24 O P3 Rh
Title of publication	Rhodium Cyclopentyl Phosphine Complexes of Wide-Bite-Angle Ligands DPEphos and Xantphos
Authors of publication	Dallanegra, Romaeo; Chaplin, Adrian B.; Weller, Andrew S.
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	7
Pages of publication	2720
a	13.4238 ± 0.0001 Å
b	14.2954 ± 0.0001 Å
c	20.7081 ± 0.0002 Å
α	73.4829 ± 0.0004°
β	84.0057 ± 0.0004°
γ	83.9868 ± 0.0004°
Cell volume	3777.28 ± 0.05 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0427
Residual factor for significantly intense reflections	0.0329
Weighted residual factors for significantly intense reflections	0.0748
Weighted residual factors for all reflections included in the refinement	0.0794
Goodness-of-fit parameter for all reflections included in the refinement	1.03
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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