Crystallography Open Database

Information card for entry 4077905

Preview

Coordinates	4077905.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C83 H67 B F24 O P3 Rh
Calculated formula	C83 H67 B F24 O P3 Rh
Title of publication	Rhodium Cyclopentyl Phosphine Complexes of Wide-Bite-Angle Ligands DPEphos and Xantphos
Authors of publication	Dallanegra, Romaeo; Chaplin, Adrian B.; Weller, Andrew S.
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	7
Pages of publication	2720
a	13.9956 ± 0.0001 Å
b	33.5274 ± 0.0003 Å
c	17.8616 ± 0.0002 Å
α	90°
β	108.154 ± 0.0004°
γ	90°
Cell volume	7964.09 ± 0.13 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0907
Residual factor for significantly intense reflections	0.0572
Weighted residual factors for significantly intense reflections	0.1244
Weighted residual factors for all reflections included in the refinement	0.1396
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4077905.html