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Information card for entry 4077946
Preview
Coordinates | 4077946.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H33 I N2 Ni |
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Calculated formula | C24 H33 I N2 Ni |
SMILES | [cH]12[cH]3[cH]4[cH]5[cH]1[Ni]2345(=C1N(C=CN1c1c(cccc1C(C)C)C(C)C)CCCC)I |
Title of publication | Synthesis and Catalytic Activity in Suzuki Coupling of Nickel Complexes Bearingn-Butyl- and Triethoxysilylpropyl-Substituted NHC Ligands: Toward the Heterogenization of Molecular Catalysts |
Authors of publication | Oertel, Anna Magdalena; Ritleng, Vincent; Chetcuti, Michael J. |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 7 |
Pages of publication | 2829 |
a | 8.1838 ± 0.0002 Å |
b | 10.9585 ± 0.0005 Å |
c | 15.6694 ± 0.0007 Å |
α | 99.404 ± 0.002° |
β | 91.338 ± 0.002° |
γ | 108.408 ± 0.002° |
Cell volume | 1311.22 ± 0.09 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0579 |
Residual factor for significantly intense reflections | 0.0412 |
Weighted residual factors for significantly intense reflections | 0.1081 |
Weighted residual factors for all reflections included in the refinement | 0.1153 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4077946.html
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