Information card for entry 4077953

Structure parameters

• Formula: C36 H54 Cl2 Cr P2 Pd
• Calculated formula: C36 H54 Cl2 Cr P2 Pd
• Title of publication: Synthesis and Reactivity of Palladium- and Platinum-Bridged Heterobimetallic [3]Trochrocenophanes
• Authors of publication: Braunschweig, Holger; Friedrich, Maria; Radacki, Krzysztof; Wolf, Justin
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 3027
• a: 26.3695 ± 0.0018 Å
• b: 18.7072 ± 0.0011 Å
• c: 17.5347 ± 0.0012 Å
• α: 90°
• β: 122.045 ± 0.003°
• γ: 90°
• Cell volume: 7331.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0683
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1471
• Weighted residual factors for all reflections included in the refinement: 0.1779
• Goodness-of-fit parameter for all reflections included in the refinement: 0.822
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No