Information card for entry 4077960

Structure parameters

• Formula: C53 H54 B N3 P3 Rh
• Calculated formula: C53 H51 B N3 P3 Rh
• Title of publication: Easy Access to Hydride Chemistry on a Tripodal P-Based Rhodium Scaffold
• Authors of publication: Tejel, Cristina; Geer, Ana M.; Jiménez, Sonia; López, José A.; Ciriano, Miguel A.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 7
• Pages of publication: 2895
• a: 15.7452 ± 0.0016 Å
• b: 13.4974 ± 0.0014 Å
• c: 21.886 ± 0.002 Å
• α: 90°
• β: 93.482 ± 0.002°
• γ: 90°
• Cell volume: 4642.6 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1202
• Residual factor for significantly intense reflections: 0.0751
• Weighted residual factors for significantly intense reflections: 0.1271
• Weighted residual factors for all reflections included in the refinement: 0.1433
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No