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Information card for entry 4078035
Preview
Coordinates | 4078035.cif |
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Original paper (by DOI) | HTML |
Formula | C35 H40 Cl4 Cu F6 N6 O P3 |
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Calculated formula | C35 H40 Cl4 Cu F6 N6 O P3 |
Title of publication | Tris(pyrazolyl)phosphine Oxides. Synthesis and Coordination Chemistry with Copper(I) |
Authors of publication | Tazelaar, Cornelis G. J.; Lyaskovskyy, Volodymyr; Dijk, Tom van; Broere, Daniël L. J.; Kolfschoten, Ludo A.; Khiar, Rima Osman Hassan; Lutz, Martin; Slootweg, J. Chris; Lammertsma, Koop |
Journal of publication | Organometallics |
Year of publication | 2012 |
Journal volume | 31 |
Journal issue | 8 |
Pages of publication | 3308 |
a | 11.0739 ± 0.0003 Å |
b | 12.6624 ± 0.0003 Å |
c | 15.9619 ± 0.0002 Å |
α | 102.223 ± 0.001° |
β | 106.463 ± 0.001° |
γ | 91.278 ± 0.001° |
Cell volume | 2089.69 ± 0.08 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0409 |
Residual factor for significantly intense reflections | 0.0349 |
Weighted residual factors for significantly intense reflections | 0.0887 |
Weighted residual factors for all reflections included in the refinement | 0.0937 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.032 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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