Information card for entry 4078110

Structure parameters

• Formula: C22 H36 F6 P2 Ru2 S
• Calculated formula: C22 H36 F6 P2 Ru2 S
• Title of publication: Synthesis and Reactivity of Hybrid Phosphido- and Hydrosulfido-Bridged Diruthenium Complexes: Transformations into Diruthenium and Tetraruthenium Complexes Bridged by Phosphido and Sulfido Ligands
• Authors of publication: Miyake, Yoshihiro; Moriyama, Taichi; Tanabe, Yoshiaki; Endo, Satoshi; Nishibayashi, Yoshiaki
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 3292
• a: 8.629 ± 0.002 Å
• b: 10.694 ± 0.003 Å
• c: 14.922 ± 0.003 Å
• α: 80.105 ± 0.005°
• β: 87.814 ± 0.006°
• γ: 89.707 ± 0.007°
• Cell volume: 1355.5 ± 0.6 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.1079
• Weighted residual factors for all reflections included in the refinement: 0.2342
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No