Information card for entry 4078466

Structure parameters

• Formula: C25.5 H43 Cl2 O4 Os P
• Calculated formula: C25.5 H43 Cl2 O4 Os P
• Title of publication: Reactions of an Osmium(IV) Complex with Allenedienes: Coordination and Intramolecular Cycloadditions
• Authors of publication: Collado, Alba; Esteruelas, Miguel A.; Gulías, Moisés; Mascareñas, José L.; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 12
• Pages of publication: 4450
• a: 8.989 ± 0.002 Å
• b: 11.663 ± 0.003 Å
• c: 14.432 ± 0.003 Å
• α: 107.341 ± 0.003°
• β: 101.738 ± 0.004°
• γ: 90.621 ± 0.004°
• Cell volume: 1409.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0837
• Weighted residual factors for all reflections included in the refinement: 0.092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No